Carbon Nanotube Dispersion with a Three Roll Mill

Carbon nanotubes (CNTs) are among the most powerful functional additives in advanced materials engineering.

Why Controlled Sheer Matters

Carbon nanotubes (CNTs) are among the most powerful functional additives in advanced materials engineering. With exceptional electrical conductivity, mechanical strength, and high aspect ratio, CNTs enable performance breakthroughs in:

  • Battery electrode slurries

  • Conductive inks and printed electronics

  • EMI shielding coatings

  • Structural conductive composites

However, realizing these properties depends on one critical factor:

Dispersion quality.

Poor dispersion destroys performance. Controlled shear unlocks it.

This is where the EXAKT Three Roll Mill becomes a strategic tool rather than just a mixing device.

Why Carbon Nanotube Dispersion Is So Challenging

CNTs do not arrive ready to perform.

They are typically supplied as tangled, highly agglomerated bundles held together by strong van der Waals forces. These forces cause nanotubes to:

  • Aggressively re-bundle

  • Resist wetting in most resin systems

  • Form conductive “dead zones”

  • Create rheology instability

If agglomerates are not properly broken down:

  • Electrical conductivity drops

  • Percolation thresholds increase

  • Mechanical reinforcement is reduced

  • Material costs rise due to overloading CNT content

In high-value systems, especially lithium-ion battery slurries or conductive coatings, improper dispersion directly affects performance, consistency, and margin.

CNT processing is not simply “mixing.”
It is microstructure engineering.

Controlled Shear vs. High-Energy Mixing

Many processors attempt CNT dispersion using bead mills, rotor-stator systems, or high-speed mixers. While these methods can reduce agglomerate size, they introduce risks:

  • Over-fragmentation of nanotubes

  • Excess heat generation

  • Media contamination

  • Limited repeatability

  • Broad particle size distribution

CNT performance depends on maintaining aspect ratio. Excessive impact energy can shorten nanotubes and disrupt conductive network formation.

A Three Roll Mill operates on a fundamentally different mechanical principle.

Instead of a chaotic impact, it applies precisely controlled, progressive shear between three horizontally aligned rolls.

 

How the Shear Mechanism Works

Material passes sequentially through:

  1. Feed roll

  2. Center roll

  3. Apron roll

Each roll rotates at increasing speed, creating a defined shear gradient. Adjustable roll gaps — often in the micron range — allow operators to dial in shear intensity with precision.

This enables:

  • Deagglomeration of CNT bundles

  • Uniform distribution throughout the matrix

  • Preservation of nanotube aspect ratio

  • Stable rheological behavior

  • Repeatable batch-to-batch performance

Rather than brute force energy, the process relies on gap-controlled shear refinement. 

Where Three Roll Mills Create Competitive Advantage

CNT dispersion is not a laboratory curiosity. It is a scale-up challenge with direct commercial impact.

 

1. Energy Storage (Battery Electrode Slurries)

Uniform CNT distribution creates more effective conductive pathways in cathode and anode formulations. The result:

  • Lower internal resistance

  • Improved rate capability

  • Reduced inactive material loading

  • Better cycle performance

Even slight improvements in conductive network formation can yield measurable gains in battery efficiency.

 

2. Conductive Inks & Printed Electronics

In screen printing, gravure, or inkjet applications, dispersion quality determines:

  • Line consistency

  • Predictable sheet resistance

  • Print resolution

  • Rheological stability

Agglomerates lead to clogging, inconsistent conductivity, and rejected batches. Controlled shear enables the uniformity required for high-precision printed electronics.

 

3. EMI Shielding & Advanced Coatings

EMI shielding systems depend on network continuity. A Three Roll Mill helps achieve:

  • Lower CNT loading to reach the percolation threshold

  • Cost savings from reduced filler use

  • Improved film uniformity

Lower filler loadings also maintain mechanical properties and reduce weight.

 

4. Advanced Structural Composites

In structural conductive composites, proper CNT dispersion:

  • Enhances mechanical reinforcement

  • Improves fracture resistance

  • Reduces defect concentration

Poor dispersion creates stress concentrators. Controlled shear mitigates that risk. 

 

5. R&D to Production Scale-Up

One of the strongest advantages of the Three Roll Mill platform is scalability.

Formulation scientists can:

  • Precisely adjust roll gaps

  • Document shear conditions

  • Reproduce dispersion parameters

  • Transition from lab to pilot to production

This controlled, measurable process environment supports predictable scale-up — critical in high-value advanced material development. 

 

Why the EXAKT Three Roll Mill Platform Is Engineered for CNT Processing

EXAKT systems are designed for precision dispersion applications, not general-purpose mixing.

Key technical advantages include:

  • Micron-level roll gap adjustment

  • Progressive shear refinement

  • Repeatable operating parameters

  • Minimal contamination risk

  • Controlled thermal impact

When processing CNTs, the objective is not maximum energy input. It is an optimized shear application.

For formulators working in conductive systems, that distinction directly impacts performance, yield, and cost efficiency.

Explore the EXAKT Three Roll Mill product line here:
https://exaktusa.com/three-roll-mill-products/

 

Final Perspective: Dispersion as a Strategic Differentiator

In advanced materials markets, dispersion quality separates commodity processing from engineered performance.

With CNT systems:

  • Shear control matters more than brute force

  • Microstructure determines conductivity

  • Repeatability drives commercial success

A Three Roll Mill does not simply blend materials.
It allows you to engineer dispersion with intent.

If you are developing CNT-based formulations and want to optimize conductivity, rheology, and material efficiency, a controlled shear platform should be part of your evaluation process.

EXAKT Three Roll Mills for CNT

Contact us today!